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Thermal decomposition of lanthanum(III) butyrate in argon atmosphere

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Authors:
  • Grivel, Jean-Claude ;
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    Orcid logo0000-0001-7835-9054
    Department of Energy Conversion and Storage, Technical University of Denmark
  • Yue, Zhao ;
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    Electrofunctional materials, Department of Energy Conversion and Storage, Technical University of Denmark
  • Xiao, Tang ;
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    Department of Energy Conversion and Storage, Technical University of Denmark
  • Pallewatta, Pallewatta G A P ;
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    Department of Energy Conversion and Storage, Technical University of Denmark
  • Watenphul, A. ;
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    Deutsches Elektronen-Synchrotron
  • Zimmermann, M.v.
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    Deutsches Elektronen-Synchrotron
DOI:
10.1016/j.tca.2013.05.016
Abstract:
The thermal decomposition of La(C3H7CO2)3·xH2O (x≈0.82) was studied in argon during heating at 5K/min. After the loss of bound H2O, the anhydrous butyrate presents at 135°C a phase transition to a mesophase, which turns to an isotropic liquid at 180°C. The decomposition of the anhydrous butyrate is associated to a solidification process. The final decomposition to La2O3 takes place via two intermediate products: La2O(C3H7CO2)4 and La2O2CO3 with release of CO2 and the symmetrical ketone C3H7COC3H7.
Type:
Journal article
Language:
English
Published in:
Thermochimica Acta, 2013, Vol 566, p. 112-117
Keywords:
Lanthanum; Butyrate; Thermal decomposition; TG/DTA; FTIR
Main Research Area:
Science/technology
Publication Status:
Published
Review type:
Peer Review
Submission year:
2013
Scientific Level:
Scientific
ID:
243640615

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